sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate

Base Information

• Chemical Name: sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate
• CAS No.: 119155-00-9
• Molecular Formula: C₁₅H₁₄N₃O₆*Na
• Molecular Weight: 355.282

Synonyms:sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate

Chemical Property of sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate

Chemical Property:

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Technology Process of sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate

There total 3 articles about sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4-nitrobenzyl 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate (119154-99-3) → sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate (119155-00-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; Ambient temperature;

DOI:10.1016/S0040-4020(01)85956-1

Reference yield:

2-oxo-glutaric acid 1-p-nitrobenzyl ester (108049-92-9) → sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate (119155-00-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 54 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

2: 79 percent / hydrogen / 10percent Pd-C / tetrahydrofuran; H₂O / Ambient temperature

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/S0040-4020(01)85956-1

Reference yield:

4-benzamidopyrazolidin-3-one (99056-13-0) → sodium 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate (119155-00-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 54 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

2: 79 percent / hydrogen / 10percent Pd-C / tetrahydrofuran; H₂O / Ambient temperature

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/S0040-4020(01)85956-1

upstream raw materials:

4-nitrobenzyl 8-benzamido-2-hydroxyl-5,9-dioxo-1,6-diazabicyclo<4.3.0>nonane-2-carboxylate

2-oxo-glutaric acid 1-p-nitrobenzyl ester

4-benzamidopyrazolidin-3-one

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