C₂₃H₂₈O₆

Base Information

Chemical Name:C₂₃H₂₈O₆
CAS No.:1352550-84-5
Molecular Formula:C₂₃H₂₈O₆
Molecular Weight:400.472
Hs Code.:

C<sub>23</sub>H<sub>28</sub>O<sub>6</sub>

Synonyms:C₂₃H₂₈O₆

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Chemical Property of C₂₃H₂₈O₆

Chemical Property:

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Technology Process of C₂₃H₂₈O₆

There total 6 articles about C₂₃H₂₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352550-81-2
C₁₆H₂₂O₄

: 1352550-84-5
C₂₃H₂₈O₆

Guidance literature:: Multi-step reaction with 5 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 1 h / 40 °C

2: sodium acetate; toluene-4-sulfonic acid hydrazide / 1,2-dimethoxyethane / 80 °C

3: Dess-Martin periodane / dichloromethane / 20 °C

4: potassium hexamethylsilazane / tetrahydrofuran / -78 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; barium(II) hydroxide / 1,2-dimethoxyethane; water / 70 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; potassium hexamethylsilazane; Dess-Martin periodane; toluene-4-sulfonic acid hydrazide; barium(II) hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; 1: ring-closure metathesis / 5: Suzuki coupling;
DOI:10.1016/j.tetlet.2011.10.145

Reference yield:

: 1352550-82-3
2-methoxy-1-(methoxymethoxy)-6,9-dihydro-5H-benzo[7]annulen-5-ol

: 1352550-84-5
C₂₃H₂₈O₆

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate; toluene-4-sulfonic acid hydrazide / 1,2-dimethoxyethane / 80 °C

2: Dess-Martin periodane / dichloromethane / 20 °C

3: potassium hexamethylsilazane / tetrahydrofuran / -78 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; barium(II) hydroxide / 1,2-dimethoxyethane; water / 70 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; potassium hexamethylsilazane; Dess-Martin periodane; toluene-4-sulfonic acid hydrazide; barium(II) hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; 4: Suzuki coupling;
DOI:10.1016/j.tetlet.2011.10.145

Reference yield:

: 1247734-18-4
2-allyl-4-methoxy-3-(methoxymethoxy)benzaldehyde

: 1352550-84-5
C₂₃H₂₈O₆

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / -78 °C

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 1 h / 40 °C

3: sodium acetate; toluene-4-sulfonic acid hydrazide / 1,2-dimethoxyethane / 80 °C

4: Dess-Martin periodane / dichloromethane / 20 °C

5: potassium hexamethylsilazane / tetrahydrofuran / -78 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; barium(II) hydroxide / 1,2-dimethoxyethane; water / 70 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; potassium hexamethylsilazane; Dess-Martin periodane; toluene-4-sulfonic acid hydrazide; barium(II) hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; 2: ring-closure metathesis / 6: Suzuki coupling;
DOI:10.1016/j.tetlet.2011.10.145