3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate

Base Information

• Chemical Name: 3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate
• CAS No.: 1618700-71-2
• Molecular Formula: C₂₈H₄₃N₃O₈
• Molecular Weight: 549.665
• Mol file: 1618700-71-2.mol

Synonyms:3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate

Chemical Property of 3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate

There total 1 articles about 3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

1,2-di-tert-butoxycarbonylpyrazolidine-3-carboxylic acid (1397581-95-1) + (S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol (66605-57-0) → 3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate (1618700-71-2) + 3-(2-(tert-butoxycarbonylamino)-3-phenylpropyl) 1,2-di-tert-butyl pyrazolidine-1,2,3-tricarboxylate (1618700-59-6)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 4 ℃; for 4h; Overall yield = 87 %; Overall yield = 6.7 mg; Inert atmosphere;

DOI:10.1080/00397911.2014.905601

upstream raw materials:

1,2-di-tert-butoxycarbonylpyrazolidine-3-carboxylic acid

(S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol