Pyoc-Phe-Leu-Leu-OtBu

Base Information

Chemical Name:Pyoc-Phe-Leu-Leu-OtBu
CAS No.:87136-66-1
Molecular Formula:C₃₃H₄₈N₄O₆
Molecular Weight:596.767
Hs Code.:

Synonyms:Pyoc-Phe-Leu-Leu-OtBu

Suppliers and Price of Pyoc-Phe-Leu-Leu-OtBu

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Pyoc-Phe-Leu-Leu-OtBu

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Pyoc-Phe-Leu-Leu-OtBu

There total 5 articles about Pyoc-Phe-Leu-Leu-OtBu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 17389-05-8
leucine tert-butylester

: 87136-65-0
Pyoc-Phe-Leu-OH

: 87136-66-1
Pyoc-Phe-Leu-Leu-OtBu

Guidance literature:: With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In dichloromethane;

Reference yield:

: 103-74-2
2-(2-Hydroxyethyl)pyridine

: 87136-66-1
Pyoc-Phe-Leu-Leu-OtBu

Guidance literature:: Multi-step reaction with 5 steps

2: acetonitrile; H₂O / 1) pH 9.5; 2) pH 6

3: 1) triethylamine, chloroformic acid ethylester / 1) CH₂Cl₂, -15 deg C; 2 h, 0 deg C; 2) -15 deg C

4: 88 percent / trifluoroacetic acid / CH₂Cl₂ / 0 °C

5: 95 percent / DCC/ HO-SU / CH₂Cl₂

With 1-hydroxy-pyrrolidine-2,5-dione; chloroformic acid ethyl ester; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; water; acetonitrile;

Reference yield:

: 87136-59-2
Pyoc-Phe-OH

: 87136-66-1
Pyoc-Phe-Leu-Leu-OtBu

Guidance literature:: Multi-step reaction with 3 steps

1: 1) triethylamine, chloroformic acid ethylester / 1) CH₂Cl₂, -15 deg C; 2 h, 0 deg C; 2) -15 deg C

2: 88 percent / trifluoroacetic acid / CH₂Cl₂ / 0 °C

3: 95 percent / DCC/ HO-SU / CH₂Cl₂

With 1-hydroxy-pyrrolidine-2,5-dione; chloroformic acid ethyl ester; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;