diethyl 1-(3-triisopropylsiloxy-5,5-dimethyl-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

Base Information

• Chemical Name: diethyl 1-(3-triisopropylsiloxy-5,5-dimethyl-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate
• CAS No.: 386746-39-0
• Molecular Formula: C₂₇H₄₆O₅Si
• Molecular Weight: 478.745
• Mol file: 386746-39-0.mol

Synonyms:diethyl 1-(3-triisopropylsiloxy-5,5-dimethyl-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

Chemical Property of diethyl 1-(3-triisopropylsiloxy-5,5-dimethyl-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of diethyl 1-(3-triisopropylsiloxy-5,5-dimethyl-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

There total 1 articles about diethyl 1-(3-triisopropylsiloxy-5,5-dimethyl-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

5,5-dimethlycyclohex-2-en-1-one (4694-17-1) + triisopropylsilyl trifluoromethanesulfonate (80522-42-5) + Sodium; (E)-1-ethoxy-2-ethoxycarbonyl-pent-1-en-4-yn-1-olate → diethyl 1-(3-triisopropylsiloxy-5,5-dimethyl-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate (386746-39-0)

Guidance literature:

In tetrahydrofuran; at 0 ℃;

DOI:10.1021/ol016718g

upstream raw materials:

5,5-dimethlycyclohex-2-en-1-one

triisopropylsilyl trifluoromethanesulfonate