tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate

Base Information

Chemical Name:tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate
CAS No.:1454771-27-7
Molecular Formula:C₁₈H₂₇NO₅
Molecular Weight:337.416
Hs Code.:

Synonyms:tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate

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Chemical Property of tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate

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Technology Process of tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate

There total 7 articles about tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 151671-03-3
tert-butyl (2R,3R,αR)-3--2-hydroxy-3-phenylpropionate

: 1454771-27-7
tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate

Guidance literature:: With 10 wt% Pd(OH)2 on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 15h; under 3800.26 Torr;
DOI:10.1016/j.tet.2013.08.007

Reference yield: 66.0%

: C₁₉H₂₆N₂O₅

: 1454771-27-7
tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate

Guidance literature:: With L-Selectride; In tetrahydrofuran; at 0 ℃;
DOI:10.1021/acscatal.9b03394

Reference yield:

: C₁₅H₁₇NO₅

: 1454771-27-7
tert-butyl (R,R)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: C₁₉H₂₈N₄O₂S / toluene / 24 h / -40 °C

2: palladium on activated charcoal; hydrogen / ethyl acetate / 760.05 Torr

3: L-Selectride / tetrahydrofuran / 0 °C

With palladium on activated charcoal; C₁₉H₂₈N₄O₂S; hydrogen; L-Selectride; In tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1021/acscatal.9b03394