C₃₇H₃₈O₈

Base Information

Chemical Name:C₃₇H₃₈O₈
CAS No.:1186304-29-9
Molecular Formula:C₃₇H₃₈O₈
Molecular Weight:610.704
Hs Code.:

C<sub>37</sub>H<sub>38</sub>O<sub>8</sub>

Synonyms:C₃₇H₃₈O₈

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Chemical Property of C₃₇H₃₈O₈

Chemical Property:

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Technology Process of C₃₇H₃₈O₈

There total 13 articles about C₃₇H₃₈O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-59-0
isovanillin

: 1186304-29-9
C₃₇H₃₈O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetra-N-butylammonium tribromide; orthoformic acid triethyl ester / 6 h / 65 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 165 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C

4.1: acetonitrile / 6 h / Reflux

4.2: 12 h / Reflux

5.1: 18-crown-6 ether; potassium carbonate / dichloromethane / 24 h / Reflux

With sodium tetrahydroborate; 18-crown-6 ether; tetra-N-butylammonium tribromide; potassium carbonate; orthoformic acid triethyl ester; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 5.1: Wittig reaction;
DOI:10.1002/ejoc.201001023

Reference yield:

: 1186304-21-1
2-(2-bromo-5-methoxyphenyl)-1,3-dioxane

: 1186304-29-9
C₃₇H₃₈O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

1.2: -78 - 20 °C

1.3: 20 °C

2.1: magnesium sulfate / dichloromethane / 12 h / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 16 h / Inert atmosphere; Reflux

4.1: 18-crown-6 ether; potassium carbonate / dichloromethane / 24 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 18-crown-6 ether; sodium carbonate; magnesium sulfate; potassium carbonate; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 3.1: Suzuki coupling / 4.1: Wittig reaction;
DOI:10.1002/ejoc.201001023

Reference yield:

: 1186304-18-6
5-(1,3-dioxan-2-yl)-2-methoxyphenol

: 1186304-29-9
C₃₇H₃₈O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 165 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C

3.1: acetonitrile / 6 h / Reflux

3.2: 12 h / Reflux

4.1: 18-crown-6 ether; potassium carbonate / dichloromethane / 24 h / Reflux

With sodium tetrahydroborate; 18-crown-6 ether; potassium carbonate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 4.1: Wittig reaction;
DOI:10.1002/ejoc.201001023