3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene

Base Information

Chemical Name:3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene
CAS No.:1391086-22-8
Molecular Formula:C₅₄H₆₆S₆
Molecular Weight:907.514
Hs Code.:

Synonyms:3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene

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Chemical Property of 3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene

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Technology Process of 3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene

There total 9 articles about 3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1391086-20-6
2,6-dibromo-3,7-bis(dodecylthio)benzo[1,2-b:4,5-b']dithiophene

: 137937-89-4
tri-n-butyl(5-phenylthiophen-2-yl)stannane

: 1391086-22-8
3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; toluene; at 85 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c3ra41822g

Reference yield:

: di(2-ethylhexyl) 3,7-bis(dodecylthio)benzo[1,2-b; 4,5-b']dithiophene-2,6-dicarboxylate

: 1391086-22-8
3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide; water / ethanol / 10 h / 100 °C

2: silver(I) acetate; potassium carbonate / 7 h / 160 °C / Inert atmosphere

3: acetic acid; N-Bromosuccinimide / 3 h / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide; toluene / 24 h / 85 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; silver(I) acetate; potassium carbonate; acetic acid; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; toluene; 4: |Migita-Sano Synthesis;
DOI:10.1039/c3ra41822g

Reference yield:

: 1391086-15-9
3,7-bis(dodecylthio)benzo[1,2-b;4,5-b']dithiophene-2,6-dicarboxylic acid

: 1391086-22-8
3,7-bis(dodecylthio)-2,6-(5-phenyl-2-thienyl)benzo[1,2-b;4,5-b']dithiophene

Guidance literature:: Multi-step reaction with 3 steps

1: silver(I) acetate; potassium carbonate / 7 h / 160 °C / Inert atmosphere

2: acetic acid; N-Bromosuccinimide / 3 h / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide; toluene / 24 h / 85 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(I) acetate; potassium carbonate; acetic acid; In N,N-dimethyl-formamide; toluene; 3: |Migita-Sano Synthesis;
DOI:10.1039/c3ra41822g