C₄₆H₆₅NO₆Si

Base Information

Chemical Name:C₄₆H₆₅NO₆Si
CAS No.:1323858-63-4
Molecular Formula:C₄₆H₆₅NO₆Si
Molecular Weight:756.111
Hs Code.:

C<sub>46</sub>H<sub>65</sub>NO<sub>6</sub>Si

Synonyms:C₄₆H₆₅NO₆Si

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Chemical Property of C₄₆H₆₅NO₆Si

Chemical Property:

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Technology Process of C₄₆H₆₅NO₆Si

There total 12 articles about C₄₆H₆₅NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 1323858-23-6
C₃₇H₄₈O₆Si

: 1323858-63-4
C₄₆H₆₅NO₆Si

Guidance literature:: With ferrous(II) sulfate heptahydrate; In methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201101893

Reference yield:

: 1323858-52-1
C₃₇H₅₀O₅Si

: 1323858-63-4
C₄₆H₆₅NO₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: [bis(acetoxy)iodo]benzene; iodine / cyclohexane / 1 h / Irradiation

2: pyridinium p-toluenesulfonate / 20 - 130 °C

3: methanol; triethylamine / 14 h / 50 °C

4: triethylamine / dichloromethane / 3 h / 0 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

6: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 0.5 h / 0 °C / Irradiation

7: ferrous(II) sulfate heptahydrate / methanol / 1 h / 20 °C / Inert atmosphere

With methanol; ferrous(II) sulfate heptahydrate; lithium aluminium tetrahydride; [bis(acetoxy)iodo]benzene; iodine; oxygen; pyridinium p-toluenesulfonate; 5,15,10,20-tetraphenylporphyrin; triethylamine; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; 6: Schenck ene reaction;
DOI:10.1002/anie.201101893

Reference yield:

: 1323858-56-5
C₃₉H₅₀O₆Si

: 1323858-63-4
C₄₆H₆₅NO₆Si

Guidance literature:: Multi-step reaction with 5 steps

1: methanol; triethylamine / 14 h / 50 °C

2: triethylamine / dichloromethane / 3 h / 0 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

4: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 0.5 h / 0 °C / Irradiation

5: ferrous(II) sulfate heptahydrate / methanol / 1 h / 20 °C / Inert atmosphere

With methanol; ferrous(II) sulfate heptahydrate; lithium aluminium tetrahydride; oxygen; 5,15,10,20-tetraphenylporphyrin; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 4: Schenck ene reaction;
DOI:10.1002/anie.201101893