C₄₂H₄₈N₅O₁₄P

Base Information

Chemical Name:C₄₂H₄₈N₅O₁₄P
CAS No.:1608113-93-4
Molecular Formula:C₄₂H₄₈N₅O₁₄P
Molecular Weight:877.842
Hs Code.:

C<sub>42</sub>H<sub>48</sub>N<sub>5</sub>O<sub>14</sub>P

Synonyms:C₄₂H₄₈N₅O₁₄P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₂H₄₈N₅O₁₄P

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Technology Process of C₄₂H₄₈N₅O₁₄P

There total 11 articles about C₄₂H₄₈N₅O₁₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1608114-11-9
N-For-Gly-L-Glu-L-Phe-OMe

: 1608113-64-9
C₂₄H₂₈N₃O₈P

: 1608113-93-4
C₄₂H₄₈N₅O₁₄P

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201301781

Reference yield:

: C₁₆H₂₃N₃O₈

: 1608113-93-4
C₄₂H₄₈N₅O₁₄P

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 2.25 h / 0 - 20 °C / Inert atmosphere

3: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301781

Reference yield:

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 1608113-93-4
C₄₂H₄₈N₅O₁₄P

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine; dmap / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

2.1: triethylamine; methanesulfonyl chloride / 2 h / 20 °C / Inert atmosphere

2.2: 1.5 h / Inert atmosphere; Reflux

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 2 h / 0 - 20 °C / Inert atmosphere

4.1: acetic acid / 3 h / 20 °C / Inert atmosphere

5.1: 1H-tetrazole / dichloromethane; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

5.2: 2 h / -40 - 20 °C / Inert atmosphere

6.1: methylamine / water; ethanol / 0.5 h / 0 - 20 °C

7.1: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C / Inert atmosphere

With 1H-tetrazole; dmap; di-isopropyl azodicarboxylate; acetic acid; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; methylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: |Mitsunobu Displacement;
DOI:10.1002/ejoc.201301781