4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne

Base Information

Chemical Name:4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne
CAS No.:1246344-59-1
Molecular Formula:C₆₉H₅₆O₃S₃
Molecular Weight:1029.4
Hs Code.:

Synonyms:4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne

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Technology Process of 4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne

There total 1 articles about 4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1246344-58-0
trimethyl[4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethynyl]silane

: 1246344-59-1
4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c002657c

Reference yield: 8.0%

: 1009039-84-2
(E)-1-(4-bromophenyl)-2-[4-[(trimethylsilyl)ethynyl]phenyl]diazene

: 1246344-59-1
4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethyne

: (E)-1-[4-[3,5,7-tris-[4-(4-acetylsulfanylmethylphenylethynyl)phenyl]adamantan-1-yl]phenylethynyl]-2-[4-[(trimethylsilyl)ethynyl]phenyl]diazene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; In tetrahydrofuran; for 96h; Inert atmosphere; Reflux;
DOI:10.1039/c002657c