5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene

Base Information

• Chemical Name: 5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene
• CAS No.: 850881-17-3
• Molecular Formula: C₇₄H₈₂INO₂S₄
• Molecular Weight: 1272.64

Synonyms:5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene

Chemical Property of 5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene

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Technology Process of 5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene

There total 1 articles about 5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-2,2';5',2'';5'',2'''-quaterthiophene → 5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene (850881-17-3)

Guidance literature:

5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-2,2';5',2'';5'',2'''-quaterthiophene; With mercury caproate; In dichloromethane; at 20 ℃;

With iodine; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1039/b414817g

Reference yield: 79.0%

5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene (850881-17-3) → 8,8'-(4,3'3,3',4,4',4,4'-octahexyl-2,2':5',2:5,2':5',2:5,2':5',2:5,2'-octithiene-5,5'-diyl)bis[2-(2,6-diisopropylphenyl)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione]

Guidance literature:

With tri-tert-butyl phosphine; caesium carbonate; hydroquinone; palladium diacetate; In N,N-dimethyl acetamide; at 80 ℃; for 24h;

DOI:10.1002/ejoc.200500147

Reference yield: 75.0%

5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3'''-tetrahexyl-5'''-iodo-2,2';5',2'';5'',2'''-quaterthiophene (850881-17-3) + 5-(4,3'-dihexyl-2,2'-bithienyl-5-yl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane (850881-12-8) → 5-([N-(2,6-diisopropylphenyl)]-9-perylenyl-3,4-dicarboximide)-4,3',3'',3''',3'''',3'''''-hexahexyl-2,2';5',2'';5'',2''';5''',2'''';5'''',2'''''-sexithiophene

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 60 ℃; for 4h;

DOI:10.1039/b414817g

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