2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid

Base Information

Chemical Name:2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid
CAS No.:92172-76-4
Molecular Formula:C₁₉H₂₀ClN₃O₃*2H₃O₄P
Molecular Weight:569.829
Hs Code.:

Synonyms:2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid

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Chemical Property of 2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid

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Technology Process of 2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid

There total 5 articles about 2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 92172-68-4
(2-Chloro-6,7-dimethoxy-8-nitro-quinolin-3-ylmethyl)-(4-methoxy-phenyl)-amine

: 92172-76-4
2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid

Guidance literature:: With hydrogen; nickel; In methanol; for 1h; under 1838.8 Torr;

Reference yield:

: 68236-23-7
2-chloro-6,7-dimethoxy-3-quinolinecarboxaldehyde

: 92172-76-4
2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / fuming nitric acid

2: 97 percent / sodium borohydride / methanol

3: 90 percent / PBr₃, triethylamine / benzene / 5 h / Heating

4: 67 percent / triethylamine / ethanol / 4 h / Heating

5: 85 percent / H₂ / Raney Nickel (10percent) / methanol / 1 h / 1838.8 Torr

With sodium tetrahydroborate; hydrogen; nitric acid; phosphorus tribromide; triethylamine; nickel; In methanol; ethanol; benzene;

Reference yield:

: 92172-65-1
3-bromomethyl-2-chloro-6,7-dimethoxy-8-nitroquinoline

: 92172-76-4
2-Chloro-6,7-dimethoxy-3-[(4-methoxy-phenylamino)-methyl]-quinolin-8-ylamine; compound with phosphoric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / triethylamine / ethanol / 4 h / Heating

2: 85 percent / H₂ / Raney Nickel (10percent) / methanol / 1 h / 1838.8 Torr

With hydrogen; triethylamine; nickel; In methanol; ethanol;