benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide

Base Information

Chemical Name:benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide
CAS No.:910127-48-9
Molecular Formula:C₁₅H₁₅NO₂S
Molecular Weight:273.356
Hs Code.:

Synonyms:benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide

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Chemical Property of benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide

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Technology Process of benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide

There total 3 articles about benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 910127-47-8
benzo[b]thiophene-2-carboxylic acid 4-hydroxycyclohexyl amide

: 910127-48-9
benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2006.05.025

Reference yield:

: 6314-28-9
benzo[b]thiophene-2-carboxylic acid

: 910127-48-9
benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / O-benzotriazol-1-yl-N,N,N',N'-tetramethyluronium BF₄; N-ethyldiisopropylamine / CH₂Cl₂; dimethylformamide / 1 h / 20 °C

2: 56 percent / 1-hydroxy-1,2-benziodoxol-3(1H)-on-1-oxide / dimethylsulfoxide / 1 h / 20 °C

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.05.025

Reference yield:

: 27489-62-9
trans-4-hydroxycyclohexylamine

: 910127-48-9
benzo[b]thiophene-2-carboxylic acid 4-oxocyclohexyl amide

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / O-benzotriazol-1-yl-N,N,N',N'-tetramethyluronium BF₄; N-ethyldiisopropylamine / CH₂Cl₂; dimethylformamide / 1 h / 20 °C

2: 56 percent / 1-hydroxy-1,2-benziodoxol-3(1H)-on-1-oxide / dimethylsulfoxide / 1 h / 20 °C

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.05.025