2-BROMO-N-(2-METHYLPHENYL)ACETAMIDE

Base Information

• Chemical Name: 2-BROMO-N-(2-METHYLPHENYL)ACETAMIDE
• CAS No.: 5332-69-4
• Molecular Formula: C9H10 Br N O
• Molecular Weight: 228.088
• Hs Code.: 2924299090
• Mol file: 5332-69-4.mol

Synonyms:o-Acetotoluidide,2-bromo- (8CI); 2-Bromo-2'-methylacetanilide; 2-Bromo-o-acetotoluidide;N-(Bromoacetyl)-2-methylaniline; NSC 547

Chemical Property of 2-BROMO-N-(2-METHYLPHENYL)ACETAMIDE

Chemical Property:

• Vapor Pressure: 9.31E-05mmHg at 25°C
• Boiling Point: 339.2°Cat760mmHg
• Flash Point: 159°C
• PSA: 29.10000
• Density: 1.5g/cm³
• LogP: 2.40140
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-N-(2-methylphenyl)acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-BROMO-N-(2-METHYLPHENYL)ACETAMIDE

There total 2 articles about 2-BROMO-N-(2-METHYLPHENYL)ACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-Bromoacetyl bromide (598-21-0) + o-toluidine (95-53-4) → 2-bromo-N-(2'-methylphenyl)acetamide (5332-69-4)

Guidance literature:

With pyridine; In chloroform; at 20 ℃; for 24h;

DOI:10.1021/jm050670l

Reference yield:

2-bromoacetyl chloride (22118-09-8) + o-toluidine (95-53-4) → 2-bromo-N-(2'-methylphenyl)acetamide (5332-69-4)

Guidance literature:

With dmap; In dichloromethane; at 0 - 25 ℃; for 3.5h; Inert atmosphere;

DOI:10.5935/0103-5053.20150104

Reference yield: 93.0%

2-bromo-N-(2'-methylphenyl)acetamide (5332-69-4) + 5-(1-phenylcarbamoylpiperidine)-4H-1,3,4-oxadiazole-2-thiol → 2-(5-(1-phenylcarbamoylpiperidine)-4H-1,3,4-oxadiazole-2-ylthio)-N-(2-methylphenyl)acetamide

Guidance literature:

5-(1-phenylcarbamoylpiperidine)-4H-1,3,4-oxadiazole-2-thiol; With potassium hydroxide; In ethanol; at 20 ℃; for 0.5h;

2-bromo-N-(2'-methylphenyl)acetamide; In ethanol;

DOI:10.1016/j.bioorg.2021.105243

upstream raw materials:

2-Bromoacetyl bromide

o-toluidine

2-bromoacetyl chloride

Downstream raw materials:

1,4-bis(2-methylphenyl)piperazine-2,5-dione

2-iodo-N-(o-methylphenyl)acetamide

N-(2-methylphenyl)diethylphosphonoacetamide

2-[{5-(4-nitrophenyl)-1,3,4-oxadiazole-2-yl}sulphanyl]-N-(2-methylphenyl)acetamide

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