5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one

Base Information

Chemical Name:5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one
CAS No.:1219596-68-5
Molecular Formula:C₂₇H₂₉NO₃S
Molecular Weight:447.598
Hs Code.:

Synonyms:5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one

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Chemical Property of 5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one

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Technology Process of 5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one

There total 1 articles about 5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1219596-66-3
4-methyl-N-(3-phenylprop-2-ynyl)-N-(5,5,7-trimethyl-6-oxooct-7-en-2-ynyl)benzenesulfonamide

: 1219596-68-5
5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one

Guidance literature:: With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In chlorobenzene; at 150 ℃; for 0.166667h; Inert atmosphere; Sealed tube; Microwave irradiation;
DOI:10.1021/ol100318f

Reference yield: 66.0%

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: 1219596-68-5
5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one

: (1RS,7SR,16SR)-14,14,16-trimethyl-10-[(4-methylbenzene)sulfonyl]-4,7-diphenyl-2,4,6,10-tetraazapentacyclo[5.5.5.0(1,16).0(2,6).0(8,12)]heptadec-8⁽¹²⁾-ene-3,5,15-trione

: (1RS,7SR,16RS)-14,14,16-trimethyl-10-[(4-methylbenzene)sulfonyl]-4,7-diphenyl-2,4,6,10-tetraazapentacyclo[5.5.5.0(1,16).0(2,6).0(8,12)]heptadec-8⁽¹²⁾-ene-3,5,15-trione

Guidance literature:: In dichloromethane; at 0 ℃; for 0.75h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol100318f

Reference yield: 56.0%

: 1219596-68-5
5a,7,7-trimethyl-4-phenyl-2-tosyl-2,3,5,5a,7,8-hexahydrocyclopenta[e]isoindol-6(1H)-one

: 13274-43-6
4-methyl-1,2,4-triazoline-3,5-dione

: (1RS,7SR,16SR)-4,14,14,16-tetramethyl-10-[(4-methylbenzene)sulfonyl]-7-phenyl-2,4,6,10-tetraazapentacyclo[5.5.5.0(1,16).0(2,6).0(8,12)]heptadec-8⁽¹²⁾-ene-3,5,15-trione

: (1RS,7SR,16RS)-4,14,14,16-tetramethyl-10-[(4-methylbenzene)sulfonyl]-7-phenyl-2,4,6,10-tetraazapentacyclo[5.5.5.0(1,16).0(2,6).0(8,12)]heptadec-8⁽¹²⁾-ene-3,5,15-trione

Guidance literature:: In dichloromethane; at 0 ℃; for 0.75h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol100318f