N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene

Base Information

Chemical Name:N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene
CAS No.:899799-02-1
Molecular Formula:C₁₄H₁₂BrNO₄S
Molecular Weight:370.224
Hs Code.:

Synonyms:N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene

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Chemical Property of N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene

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Technology Process of N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene

There total 1 articles about N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4277-63-8
methyl 1H-pyrrole-1-carboxylate

: 227454-52-6
[(bromoethynyl)sulfonyl]benzene

: 899799-02-1
N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene

Guidance literature:: DOI:10.1016/j.tetlet.2006.04.014

Reference yield: 100.0%

: 899799-02-1
N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene

: 899799-04-3
2-benzenesulfonyl-3-bromo-7-aza-bicyclo[2.2.1]hept-2-ene-7-carboxylic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2006.04.014

Reference yield:

: 899799-02-1
N-methoxycarbonyl-7-aza-2-bromo-3-phenylsulfonylbicyclo[2.2.1]hepta-2,5-diene

: 899799-05-4
2-benzenesulfonyl-3-phenylsulfanyl-7-aza-bicyclo[2.2.1]hept-2-ene-7-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C

2: NaH / tetrahydrofuran

With hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.tetlet.2006.04.014