dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester

Base Information

• Chemical Name: dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester
• CAS No.: 588706-83-6
• Molecular Formula: C₂₇H₂₆N₂O₅S₂
• Molecular Weight: 522.646

Synonyms:dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester

Chemical Property of dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester

Chemical Property:

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Technology Process of dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester

There total 3 articles about dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

potassium ethyl xanthogenate (140-89-6) + 4-[(E)-3-(4-Benzyloxy-3-methoxy-phenyl)-2-nitro-propenyl]-benzonitrile → dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester (588706-83-6)

Guidance literature:

In acetic acid; at 0 - 20 ℃;

DOI:10.1021/ol035027c

Reference yield:

2-(4'-benzyloxy-3'-methoxyphenyl)-1-nitroethane (21473-46-1) → dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester (588706-83-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / acetic acid; n-butylamine / toluene / 4 h / Heating

2: 80 percent / acetic acid / 0 - 20 °C

With acetic acid; N-butylamine; In acetic acid; toluene; 1: Knoevenagel reaction / 2: Michael addition;

DOI:10.1021/ol035027c

Reference yield:

4-cyanobenzaldehyde (105-07-7) → dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester (588706-83-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / acetic acid; n-butylamine / toluene / 4 h / Heating

2: 80 percent / acetic acid / 0 - 20 °C

With acetic acid; N-butylamine; In acetic acid; toluene; 1: Knoevenagel reaction / 2: Michael addition;

DOI:10.1021/ol035027c

upstream raw materials:

potassium ethyl xanthogenate

2-(4'-benzyloxy-3'-methoxyphenyl)-1-nitroethane

4-cyanobenzaldehyde

Downstream raw materials:

dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

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