C₂₇H₂₈N₂O₈

Base Information

Chemical Name:C₂₇H₂₈N₂O₈
CAS No.:1016976-43-4
Molecular Formula:C₂₇H₂₈N₂O₈
Molecular Weight:508.528
Hs Code.:

C<sub>27</sub>H<sub>28</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₂₇H₂₈N₂O₈

Suppliers and Price of C₂₇H₂₈N₂O₈

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₇H₂₈N₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₇H₂₈N₂O₈

There total 22 articles about C₂₇H₂₈N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: C₂₆H₃₀N₂O₇

: 1016976-28-5
C₂₇H₂₈N₂O₈

: 1016976-43-4
C₂₇H₂₈N₂O₈

Guidance literature:: With pyridine; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1021/ol800127a

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: C₂₆H₃₀N₂O₇

: 1016976-43-4
C₂₇H₂₈N₂O₈

Guidance literature:: With pyridine; In dichloromethane; at -78 - 0 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: 885703-19-5
(3S,4S)-4-N-phthalimido-1,5-hexadiene-3-ol

: 1016976-43-4
C₂₇H₂₈N₂O₈

Guidance literature:: Multi-step reaction with 17 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 11 h / 20 °C / Inert atmosphere

2: osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 6 h / 5 °C / Inert atmosphere

3: nitrogen; methylamine / water / 1 h / 50 °C / 10 Torr / Inert atmosphere

4: sodium hydrogencarbonate / ethyl acetate / 1.5 h / Inert atmosphere

5: dmap; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.03 h / 0 - 20 °C / Inert atmosphere

6: dichloromethane / 1 h / -40 °C / Inert atmosphere

7: caesium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

8: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / Inert atmosphere

9: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

10: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

11: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

12: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

13: dmap; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

14: 1,4-diaza-bicyclo[2.2.2]octane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine / tetrahydrofuran / 20 °C / Inert atmosphere

15: palladium diacetate; silver nitrate; triphenylphosphine / 1,4-dioxane / 1 h / 80 °C / Inert atmosphere

16: 4-methyl-morpholine; osmium(VIII) oxide / tetrahydrofuran; water; acetone / 3 h / 20 °C / Inert atmosphere

17: pyridine / dichloromethane / 0.08 h / -78 - 0 °C / Inert atmosphere

With 4-methyl-morpholine; pyridine; 1,4-diaza-bicyclo[2.2.2]octane; 1H-imidazole; dmap; osmium(VIII) oxide; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; nitrogen; tetrabutyl ammonium fluoride; palladium diacetate; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; Dess-Martin periodane; silver nitrate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; methylamine; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine; potassium hexacyanoferrate(III); In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water; ethyl acetate; N,N-dimethyl-formamide; acetone; tert-butyl alcohol; 17: Polonovski reaction;
DOI:10.1002/chem.201003489