phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside
CAS No.:612841-75-5
Molecular Formula:C₂₈H₂₈O₅S
Molecular Weight:476.593
Hs Code.:

Synonyms:phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside

There total 6 articles about phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: (2R,3S,4S,5R,6S)-4-Benzyloxy-2-hydroxymethyl-6-phenylsulfanyl-2-vinyl-tetrahydro-pyran-3,5-diol

: 612841-75-5
phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide; at 20 ℃; for 14h;
DOI:10.1016/S0040-4039(03)01631-9

Reference yield:

: 612841-73-3
1,2,4,6-tetra-O-acetyl-3-O-benzyl-5-C-vinyl-β-D-glucopyranoside

: 612841-75-5
phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / BF₃*OEt₂ / CH₂Cl₂ / 10 h / 20 °C

2: CH₃OH; sodium / 1 h / 20 °C

3: 8.28 g / camphorsulphonic acid / dimethylformamide / 14 h / 20 °C

With methanol; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.06.009

Reference yield:

: 612841-74-4
phenyl 2,4,6-tri-O-acetyl-3-O-benzyl-5-C-vinyl-1-thio-β-D-glucopyranoside

: 612841-75-5
phenyl 3-O-benzyl-4,6-O-benzylidene-5-C-vinyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: CH₃OH; sodium / 1 h / 20 °C

2: 8.28 g / camphorsulphonic acid / dimethylformamide / 14 h / 20 °C

With methanol; camphor-10-sulfonic acid; sodium; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.06.009