sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

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Chemical Name:sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate
CAS No.:100944-82-9
Molecular Formula:C₁₈H₁₆ClN₂O₄S₂*Na
Molecular Weight:446.911
Hs Code.:

Synonyms:sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

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Technology Process of sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

There total 2 articles about sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 88045-94-7
1-(α-benzylthiobenzyl)-5-chloro-2(1H)-pyrimidinone

: 100944-82-9
sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Guidance literature:: With sodium hydrogensulfite; In water; RT, 4 h; 100 deg C, 10 min, 5 deg C;

Reference yield:

: 51317-73-8
α-Chlorodibenzyl sulfide

: 100944-82-9
sodium 5-chloro-1-α-(phenylsulfenyl)benzyl-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / Et₃N / CH₂Cl₂ / 24 h / Ambient temperature

2: 97 percent / NaHSO₃ / H₂O / RT, 4 h; 100 deg C, 10 min, 5 deg C

With sodium hydrogensulfite; triethylamine; In dichloromethane; water;