C₁₅H₂₂OSi

Base Information

• Chemical Name: C₁₅H₂₂OSi
• CAS No.: 1338001-20-9
• Molecular Formula: C₁₅H₂₂OSi
• Molecular Weight: 246.425
• Mol file: 1338001-20-9.mol

Synonyms:C₁₅H₂₂OSi

Chemical Property of C₁₅H₂₂OSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₂OSi

There total 2 articles about C₁₅H₂₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-phenylhept-1-yn-3-ol (72206-40-7) + 1,1,3,3-tetramethyldisilazane (15933-59-2) → C15H22OSi (1338001-20-9)

Guidance literature:

1-phenylhept-1-yn-3-ol; 1,1,3,3-tetramethyldisilazane; at 20 ℃; for 12h; Inert atmosphere;

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1002/anie.201103886

Reference yield:

pentanal (110-62-3) → C15H22OSi (1338001-20-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: 12 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane;

DOI:10.1002/anie.201103886

Reference yield: 92.0%

C15H22OSi (1338001-20-9) + methyllithium (917-54-4) → C16H26OSi

Guidance literature:

C₁₅H₂₂OSi; methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h; Inert atmosphere;

With allyl bromide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1002/anie.201103886

upstream raw materials:

pentanal

1-phenylhept-1-yn-3-ol

1,1,3,3-tetramethyldisilazane

Downstream raw materials:

1,1-diphenyl-1-hepten-3-ol

C₁₄H₂₀O