C₃₃H₄₅BrN₂O₁₀Si

Base Information

Chemical Name:C₃₃H₄₅BrN₂O₁₀Si
CAS No.:1283742-25-5
Molecular Formula:C₃₃H₄₅BrN₂O₁₀Si
Molecular Weight:737.717
Hs Code.:

C<sub>33</sub>H<sub>45</sub>BrN<sub>2</sub>O<sub>10</sub>Si

Synonyms:C₃₃H₄₅BrN₂O₁₀Si

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Chemical Property of C₃₃H₄₅BrN₂O₁₀Si

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Technology Process of C₃₃H₄₅BrN₂O₁₀Si

There total 1 articles about C₃₃H₄₅BrN₂O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1283742-24-4
C₂₈H₃₆Br₂N₂O₁₀

: 1066-54-2
trimethylsilylacetylene

: 1283742-25-5
C₃₃H₄₅BrN₂O₁₀Si

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; In toluene; at 80 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201006084

Reference yield: 62.0%

: 1283742-25-5
C₃₃H₄₅BrN₂O₁₀Si

: 1283742-19-7
C₃₅H₄₆N₂O₁₀Si

: 1283742-26-6
C₆₈H₉₀N₄O₂₀Si₂

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; triphenylphosphine; In toluene; at 80 ℃; for 13h; Inert atmosphere;
DOI:10.1002/anie.201006084

Reference yield:

: 1283742-25-5
C₃₃H₄₅BrN₂O₁₀Si

: 1283742-19-7
C₃₅H₄₆N₂O₁₀Si

: 1283742-27-7
C₆₂H₇₄N₄O₂₀

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; triphenylphosphine / toluene / 13 h / 80 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride; water / tetrahydrofuran

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; water; diisopropylamine; triphenylphosphine; In tetrahydrofuran; toluene; 1: Sonogashira coupling;
DOI:10.1002/anie.201006084