O-(tri-iso-propylsilyl)-3-ethylphenol

Base Information

Chemical Name:O-(tri-iso-propylsilyl)-3-ethylphenol
CAS No.:1266547-45-8
Molecular Formula:C₁₇H₃₀OSi
Molecular Weight:278.51
Hs Code.:

Synonyms:O-(tri-iso-propylsilyl)-3-ethylphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(tri-iso-propylsilyl)-3-ethylphenol

Chemical Property:

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Technology Process of O-(tri-iso-propylsilyl)-3-ethylphenol

There total 1 articles about O-(tri-iso-propylsilyl)-3-ethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 13154-24-0
triisopropylsilyl chloride

: 620-17-7
3-ethylphenol

: 1266547-45-8
O-(tri-iso-propylsilyl)-3-ethylphenol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 24 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ja200034b

Reference yield: 98.0%

: 1266547-45-8
O-(tri-iso-propylsilyl)-3-ethylphenol

: 1266547-59-4
C₁₇H₃₂OSi

Guidance literature:: O-(tri-iso-propylsilyl)-3-ethylphenol; With ammonia; lithium; In tert-butyl alcohol; at -30 ℃; for 1.25h; Inert atmosphere; Reflux;

With ammonium chloride; In tert-butyl alcohol; at -78 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/ja200034b

Reference yield:

: 1266547-45-8
O-(tri-iso-propylsilyl)-3-ethylphenol

: C₁₇H₃₄O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonia; lithium / tert-butyl alcohol / 1.25 h / -30 °C / Inert atmosphere; Reflux

1.2: 0.17 h / -78 °C / Inert atmosphere

2.1: methanesulfonamide; AD-mix-α; water / tert-butyl methyl ether; tert-butyl alcohol / 40 h / -5 °C / Inert atmosphere

With methanesulfonamide; AD-mix-α; ammonia; water; lithium; In tert-butyl methyl ether; tert-butyl alcohol; 1.1: Birch reduction;
DOI:10.1021/ja200034b