2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate

Base Information

Chemical Name:2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate
CAS No.:1185745-16-7
Molecular Formula:C₂₃H₂₈O₁₃
Molecular Weight:512.468
Hs Code.:

Synonyms:2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate

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Technology Process of 2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate

There total 3 articles about 2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 69039-02-7
2-(3,4-dihydroxyphenyl)ethyl acetate

: methyl 2,3,4-tri-O-acetyl-α,β-D-glucopyranosyluronate trichloroacetimidate

: 1185745-16-7
2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -10 ℃; for 2h;
DOI:10.1016/j.carres.2009.05.016

Reference yield:

: 92420-89-8
methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 69039-02-7
2-(3,4-dihydroxyphenyl)ethyl acetate

: 1185745-16-7
2-[3′-hydroxy-4′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate

: 1185745-17-8
2-[4′-hydroxy-3′-(methyl-2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)phenyl]ethyl acetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 ℃; for 2h; Overall yield = 31 %; Overall yield = 445 mg;
DOI:10.1021/jf4016202