[Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2]

Base Information

Chemical Name:[Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2]
CAS No.:511551-38-5
Molecular Formula:C₄₄H₅₀Si₂Ti
Molecular Weight:682.932
Hs Code.:

[Ti(C<sub>5</sub>(CH<sub>3</sub>)4(Si(C<sub>6</sub>H<sub>5</sub>)2CH<sub>3</sub>))2]

Synonyms:[Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2]

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Chemical Property of [Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2]

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Technology Process of [Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2]

There total 1 articles about [Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 511551-29-4
[((C₆H₅)2Si(CH₃)C(CCH₃)4)2TiCl₂]

: 511551-38-5
[Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2]

Guidance literature:: With Mg; In tetrahydrofuran; byproducts: MgCl; high-vac. line technique; soln. of Ti complex (1 equiv.) in THF was added to Mg (1 equiv.); mixt. was stirred at 60°C for 1-3 d until Mg disappeared; volatiles distd. (vac.); residue extd. (hexane); concd.; soln. poured away; residue dissolved in toluene; concd.; cooled to -18°C; pptd.;
DOI:10.1016/S0022-328X(02)01726-6

Reference yield: 84.0%

: 511551-38-5
[Ti(C₅(CH₃)4(Si(C₆H₅)2CH₃))2]

: 511551-29-4
[((C₆H₅)2Si(CH₃)C(CCH₃)4)2TiCl₂]

Guidance literature:: With PbCl₂; In tetrahydrofuran; soln. of Ti complex (1 equiv.) in THF was poured on solid, vac.-dried PbCl2 (1 equiv.); mixt. was stirred at 60°C for 4 h; volatiles evapd. (vac.); residue extd. (hexane); concd.; cooled at -18°C overnight;
DOI:10.1016/S0022-328X(02)01726-6