N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide

Base Information

Chemical Name:N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide
CAS No.:900798-77-8
Molecular Formula:C₃₄H₄₄N₄O₃
Molecular Weight:556.748
Hs Code.:

Synonyms:N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide

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Chemical Property of N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide

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Technology Process of N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide

There total 1 articles about N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 900799-07-7
2-(allyl-methyl-amino)-6-methoxy-isonicotinic acid hydrochloride

: 900800-09-1
{(1S,2R)-1-(3-allyl-benzyl)-3-[benzyloxycarbonyl-(3-isopropyl-benzyl)-amino]-2-hydroxy-propyl}-carbamic acid tert-butyl ester

: 900798-77-8
N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide

Guidance literature:: {(1S,2R)-1-(3-allyl-benzyl)-3-[benzyloxycarbonyl-(3-isopropyl-benzyl)-amino]-2-hydroxy-propyl}-carbamic acid tert-butyl ester; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

2-(allyl-methyl-amino)-6-methoxy-isonicotinic acid hydrochloride; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 20h;

Reference yield:

: 900798-77-8
N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide

: N-[(1S,2R)-1-(3-Butyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-methoxy-6-methylamino-isonicotinamide

: 900798-00-7
(S)-4-[(R)-1-hydroxy-2-(3-isopropylbenzylamino)ethyl]-18-methoxy-15-methyl-3,15,17-triazatricyclo[14.3.1.1*6,10*]henicosa-1⁽²⁰⁾,6,8,10⁽²¹⁾,16,18-hexaen-2-one

Guidance literature:: N-[(1S,2R)-1-(3-allyl-benzyl)-2-hydroxy-3-(3-isopropyl-benzylamino)-propyl]-2-(allyl-methyl-amino)-6-methoxy-isonicotinamide; With hydrogenchloride; In 1,4-dioxane;

dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III); In dichloromethane; for 3.5h; Heating / reflux;

With hydrogen; 5%-palladium/activated carbon; In tetrahydrofuran; methanol; at 20 ℃; for 2.35h; under 760.051 Torr;