C₄₂H₇₅NO₈S

Base Information

Chemical Name:C₄₂H₇₅NO₈S
CAS No.:1431220-29-9
Molecular Formula:C₄₂H₇₅NO₈S
Molecular Weight:754.125
Hs Code.:

C<sub>42</sub>H<sub>75</sub>NO<sub>8</sub>S

Synonyms:C₄₂H₇₅NO₈S

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Chemical Property of C₄₂H₇₅NO₈S

Chemical Property:

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Technology Process of C₄₂H₇₅NO₈S

There total 18 articles about C₄₂H₇₅NO₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1431220-35-7
C₆₃H₉₃NO₈S

: 1431220-29-9
C₄₂H₇₅NO₈S

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.3998/ark.5550190.0014.224

Reference yield:

: 88303-25-7
tetradecylmagnesium bromide

: 1431220-29-9
C₄₂H₇₅NO₈S

Guidance literature:: Multi-step reaction with 12 steps

1.1: tetrahydrofuran

2.1: pyridine

3.1: toluene-4-sulfonic acid / methanol; dichloromethane

4.1: sodium azide / N,N-dimethyl-formamide / Heating

5.1: toluene-4-sulfonic acid

6.1: pyridine

7.1: lithium iodide / N,N-dimethyl-formamide

8.1: sodium hydrogencarbonate; tetra(n-butyl)ammonium hydrogensulfate / ethyl acetate

9.1: triphenylphosphine / tetrahydrofuran / 2 h / 20 °C

9.2: Staudinger Azide Reduction / 2 h

10.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

11.1: hydrogenchloride / methanol; dichloromethane; 1,4-dioxane / 2.5 h / 20 °C

12.1: sodium; ammonia / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

With pyridine; hydrogenchloride; sodium azide; ammonia; tetra(n-butyl)ammonium hydrogensulfate; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; lithium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 1.1: |Grignard Reaction / 9.1: |Staudinger Azide Reduction / 12.1: |Birch Reduction;
DOI:10.3998/ark.5550190.0014.224

Reference yield:

: 117168-59-9
(2S,3S,4R)-2-azido-1,3,4-octadecanetriol

: 1431220-29-9
C₄₂H₇₅NO₈S

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene-4-sulfonic acid

2.1: pyridine

3.1: lithium iodide / N,N-dimethyl-formamide

4.1: sodium hydrogencarbonate; tetra(n-butyl)ammonium hydrogensulfate / ethyl acetate

5.1: triphenylphosphine / tetrahydrofuran / 2 h / 20 °C

5.2: Staudinger Azide Reduction / 2 h

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

7.1: hydrogenchloride / methanol; dichloromethane; 1,4-dioxane / 2.5 h / 20 °C

8.1: sodium; ammonia / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

With pyridine; hydrogenchloride; ammonia; tetra(n-butyl)ammonium hydrogensulfate; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; lithium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 5.1: |Staudinger Azide Reduction / 8.1: |Birch Reduction;
DOI:10.3998/ark.5550190.0014.224