N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

Base Information

Chemical Name:N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine
CAS No.:920752-30-3
Molecular Formula:C₃₃H₃₃N₅O₃
Molecular Weight:547.657
Hs Code.:

<i>N</i>'-biphenyl-3-yl-<i>N</i>-(2,4-dimethoxy-benzyl)-1-oxy-<i>N</i>''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

Synonyms:N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

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Chemical Property of N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

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Technology Process of N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

There total 5 articles about N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 920752-29-0
4-bromo-N-(2,4-dimethoxy-benzyl)-1-oxy-N'-(2-pyridin-2-yl-ethyl)-pyridine-2,6-diamine

: 2243-47-2
3-biphenyl amine

: 920752-30-3
N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

Guidance literature:: With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In toluene; at 100 ℃; for 18h;
DOI:10.1016/j.tetlet.2006.10.159

Reference yield:

: 920752-28-9
(4,6-dibromo-1-oxy-pyridin-2-yl)-(2,4-dimethoxy-benzyl)-amine

: 920752-30-3
N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 2-methoxy-ethanol / 18 h / 130 °C

2: 37 percent / rac-BINAP; NaOtBu / Pd₂(dba)3 / toluene / 18 h / 100 °C

With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In 2-methoxy-ethanol; toluene; 2: Buckwald coupling;
DOI:10.1016/j.tetlet.2006.10.159

Reference yield:

: 2706-56-1
2-(aminoethyl)pyridine

: 920752-30-3
N'-biphenyl-3-yl-N-(2,4-dimethoxy-benzyl)-1-oxy-N''-(2-pyridin-2-yl-ethyl)-pyridine-2,4,6-triamine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 2-methoxy-ethanol / 18 h / 130 °C

2: 37 percent / rac-BINAP; NaOtBu / Pd₂(dba)3 / toluene / 18 h / 100 °C

With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In 2-methoxy-ethanol; toluene; 2: Buckwald coupling;
DOI:10.1016/j.tetlet.2006.10.159