Methyl-2-acetamido-3,4-di-O-benzyl-6-O-trityl-2-deoxy-β-D-glucopyranosid

Base Information

• Chemical Name: Methyl-2-acetamido-3,4-di-O-benzyl-6-O-trityl-2-deoxy-β-D-glucopyranosid
• CAS No.: 69892-51-9
• Molecular Formula: C₄₂H₄₃NO₆
• Molecular Weight: 657.807

Synonyms:Methyl-2-acetamido-3,4-di-O-benzyl-6-O-trityl-2-deoxy-β-D-glucopyranosid

Chemical Property of Methyl-2-acetamido-3,4-di-O-benzyl-6-O-trityl-2-deoxy-β-D-glucopyranosid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of Methyl-2-acetamido-3,4-di-O-benzyl-6-O-trityl-2-deoxy-β-D-glucopyranosid

There total 4 articles about Methyl-2-acetamido-3,4-di-O-benzyl-6-O-trityl-2-deoxy-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-acetyl-D-glucosamine (72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4) → N-((3R,4R,5S,6R)-4,5-Bis-benzyloxy-2-methoxy-6-trityloxymethyl-tetrahydro-pyran-3-yl)-acetamide (69892-50-8,69892-51-9,78488-32-1,78488-33-2)

Guidance literature:

Multi-step reaction with 3 steps

1: acetyl chloride

2: pyridine

3: NaOH

With pyridine; sodium hydroxide; acetyl chloride;

Reference yield:

N-((4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-methoxy-tetrahydro-pyran-3-yl)-acetamide (3055-46-7,3946-01-8,5627-24-7,6082-04-8,6082-22-0,17327-09-2,22256-76-4,32087-35-7,32087-36-8,95341-97-2,114029-61-7,114612-10-1,114612-13-4,116559-74-1) → N-((3R,4R,5S,6R)-4,5-Bis-benzyloxy-2-methoxy-6-trityloxymethyl-tetrahydro-pyran-3-yl)-acetamide (69892-50-8,69892-51-9,78488-32-1,78488-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: NaOH

With pyridine; sodium hydroxide;

Reference yield:

benzyl chloride (100-44-7) + methyl 2-acetamido-2-deoxy-6-O-trityl-D-glucopyranoside (42756-57-0,50908-05-9,69892-34-8,78488-16-1,78488-31-0) → N-((3R,4R,5S,6R)-4,5-Bis-benzyloxy-2-methoxy-6-trityloxymethyl-tetrahydro-pyran-3-yl)-acetamide (69892-50-8,69892-51-9,78488-32-1,78488-33-2)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

benzyl chloride

methyl 2-acetamido-2-deoxy-6-O-trityl-D-glucopyranoside

N-acetyl-D-glucosamine

N-((4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-methoxy-tetrahydro-pyran-3-yl)-acetamide

Downstream raw materials:

methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranoside

methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

2-acetamido-3,4-di-O-benzyl-2-deoxy-D-glucopyranoside

Acetic acid (1S,2S,3R,4R,5S,6S)-2-acetylamino-3,4-bis-benzyloxy-5-hydroxy-6-nitro-cyclohexyl ester

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