tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate

Base Information

Chemical Name:tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate
CAS No.:1150277-09-0
Molecular Formula:C₂₄H₃₇ClO₅S
Molecular Weight:473.074
Hs Code.:

Synonyms:tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate

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Chemical Property of tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate

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Technology Process of tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate

There total 1 articles about tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 938436-17-0
3,3-bis(ethoxymethyl)-1-[chloro(p-tolylsulfinyl)methylidene]cyclobutane

: 540-88-5
acetic acid tert-butyl ester

: 1150277-09-0
tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate

Guidance literature:: acetic acid tert-butyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

3,3-bis(ethoxymethyl)-1-[chloro(p-tolylsulfinyl)methylidene]cyclobutane; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.02.053

Reference yield: 90.0%

: 1150277-09-0
tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate

: 1268616-49-4
C₂₀H₃₁ClO₄S

Guidance literature:: tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate; With diisobutylaluminium hydride; In toluene; at 0 ℃; for 0.166667h; Inert atmosphere;

With hydrogenchloride; In water; toluene;
DOI:10.1016/j.tet.2010.12.023

Reference yield:

: 1150277-09-0
tert-butyl (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)acetate

: 1-(2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(ethoxymethyl)cyclobutyl)ethoxymethyl)-p-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / toluene / 0.17 h / 0 °C / Inert atmosphere

2: silver(l) oxide / ethyl acetate / 12 h / Reflux

With diisobutylaluminium hydride; silver(l) oxide; In ethyl acetate; toluene;
DOI:10.1016/j.tet.2010.12.023