N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide

Base Information

• Chemical Name: N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide
• CAS No.: 117014-30-9
• Molecular Formula: C₁₈H₁₇N₅O₅S₂
• Molecular Weight: 447.495

Synonyms:N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide

Chemical Property of N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide

Chemical Property:

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Technology Process of N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide

There total 3 articles about N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N-Acetyl-4-(3-benzyl-2-oxo-4-thioxo-thiazolidin-5-ylazo)-benzenesulfonamide (117014-22-9) → N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide (117014-30-9)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 2h; Heating;

DOI:10.1016/0223-5234(87)90287-X

Reference yield:

3-Benzylthiazolidin-2-one-4-thione (95213-81-3) → N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide (117014-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaNO₂ / 1.) acetic acid, water, 0-5 deg C, 10 min, 2.) dioxane, 0 deg C, 2 h

2: 53 percent / hydroxylamine hydrochloride, sodium acetate / ethanol / 2 h / Heating

With hydroxylamine hydrochloride; sodium acetate; sodium nitrite; In ethanol;

DOI:10.1016/0223-5234(87)90287-X

Reference yield:

sulphaacetamide (144-80-9) → N-Acetyl-4-{3-benzyl-4-[(Z)-hydroxyimino]-2-oxo-thiazolidin-5-ylazo}-benzenesulfonamide (117014-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaNO₂ / 1.) acetic acid, water, 0-5 deg C, 10 min, 2.) dioxane, 0 deg C, 2 h

2: 53 percent / hydroxylamine hydrochloride, sodium acetate / ethanol / 2 h / Heating

With hydroxylamine hydrochloride; sodium acetate; sodium nitrite; In ethanol;

DOI:10.1016/0223-5234(87)90287-X

upstream raw materials:

N-Acetyl-4-(3-benzyl-2-oxo-4-thioxo-thiazolidin-5-ylazo)-benzenesulfonamide

3-Benzylthiazolidin-2-one-4-thione

sulphaacetamide

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