10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine

Base Information

Chemical Name:10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine
CAS No.:143674-45-7
Molecular Formula:C₁₉H₁₅BiCl₂S
Molecular Weight:555.281
Hs Code.:

Synonyms:10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine

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Technology Process of 10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine

There total 2 articles about 10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 143674-27-5
10-(4'-methylphenyl)phenothiabismine

: 143674-45-7
10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine

Guidance literature:: With SO₂Cl₂; In hexane; dropwise addn. of sulfuryl dichloride in hexane to a suspn. of the phenothiabismine in hexane under Ar, stirring for 2 h; workup: pouring into cold brine; extractn. with ethyl acetate; recrystn. from hexane, elem. anal.;

Reference yield:

: 21848-84-0
1-bromo-2-[(2-bromophenyl)thio]benzene

: 143674-45-7
10,10-dichloro-10-(4'-methylphenyl)phenothia-10λ5-bismine

Guidance literature:: Multi-step reaction with 2 steps

1: C₄H₉Li / tetrahydrofuran; diethyl ether

2: SO₂Cl₂ / hexane

With C₄H₉Li; SO₂Cl₂; In tetrahydrofuran; diethyl ether; hexane;