1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea

Base Information

Chemical Name:1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea
CAS No.:1187856-32-1
Molecular Formula:C₂₂H₂₈N₂O₂
Molecular Weight:352.477
Hs Code.:

Synonyms:1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea

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Chemical Property of 1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea

Chemical Property:

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Technology Process of 1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea

There total 1 articles about 1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 554453-93-9
((1r,4r)-4-((methylamino)methyl)cyclohexyl)methanol

: 83-01-2
diphenylcarbamic chloride

: 1187856-32-1
1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea

Guidance literature:: With pyridine; at 20 ℃; Reflux;

Reference yield:

: 1187856-32-1
1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea

: 35059-50-8
t-butyl diazoacetate

: C₂₈H₃₈N₂O₄

Guidance literature:: dirhodium tetraacetate; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 1187856-32-1
1-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1-methyl-3,3-diphenylurea

: 1187856-31-0
2-(((1r,4r)-4-((1-methyl-3,3-diphenylureido)methyl)cyclohexyl)methoxy)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dirhodium tetraacetate / dichloromethane / 1 h / 0 °C

2: hydrogenchloride / 1,4-dioxane

With hydrogenchloride; dirhodium tetraacetate; In 1,4-dioxane; dichloromethane;