methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside

Base Information

Chemical Name:methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside
CAS No.:131367-30-1
Molecular Formula:C₂₅H₃₅NO₁₀
Molecular Weight:509.554
Hs Code.:

Synonyms:methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside

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Chemical Property of methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside

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Technology Process of methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside

There total 2 articles about methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 109-87-5
Dimethoxymethane

: 131367-25-4
methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-D-glycero-α-D-ido-heptoseptanoside

: 131367-30-1
methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside

Guidance literature:: With phosphorus pentoxide; In chloroform; for 4h; Ambient temperature;

Reference yield:

: 1116-98-9
cyanoacetic acid tert-butyl ester

: 131367-30-1
methyl 5,7,O-benzylidene-3-tert-butoxycarbonyl-3-C-cyano-3-deoxy-2,4-di-O-methoxymethyl-D-glycero-α-D-ido-heptoseptanoside

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / piperidine / dioxane; H₂O / 0.5 h / Ambient temperature

2: 96 percent / P₂O₅ / CHCl₃ / 4 h / Ambient temperature

With piperidine; phosphorus pentoxide; In 1,4-dioxane; chloroform; water;