3,5-dinitrobenzylamine

Base Information

Chemical Name:3,5-dinitrobenzylamine
CAS No.:771579-30-7
Molecular Formula:C₇H₇N₃O₄
Molecular Weight:197.15
Hs Code.:

Synonyms:3,5-dinitrobenzylamine

Suppliers and Price of 3,5-dinitrobenzylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-dinitrobenzylamine

Chemical Property:

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Technology Process of 3,5-dinitrobenzylamine

There total 4 articles about 3,5-dinitrobenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 444343-45-7
N-(3,5-dinitrobenzyl)phthalimide

: 771579-30-7
3,5-dinitrobenzylamine

Guidance literature:: With toluene-4-sulfonic acid; hydrazine hydrate; In tetrahydrofuran; for 2h; Reflux;
DOI:10.1021/acs.jmedchem.9b00912

Reference yield:

: 99-34-3
3,5-dinitrobenzoic acid

: 771579-30-7
3,5-dinitrobenzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / 0 - 25 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 48 h / 25 °C / Inert atmosphere

3: toluene-4-sulfonic acid; hydrazine / tetrahydrofuran / 2 h / Reflux

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; triphenylphosphine; hydrazine; In tetrahydrofuran; 2: Mitsunobu reaction;
DOI:10.1039/c0ob00455c

Reference yield:

: 71022-43-0
3,5-dinitrobenzyl alcohol

: 771579-30-7
3,5-dinitrobenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 48 h / 25 °C / Inert atmosphere

2: toluene-4-sulfonic acid; hydrazine / tetrahydrofuran / 2 h / Reflux

With di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; triphenylphosphine; hydrazine; In tetrahydrofuran; 1: Mitsunobu reaction;
DOI:10.1039/c0ob00455c