1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione

Base Information

Chemical Name:1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione
CAS No.:119507-80-1
Molecular Formula:C₄₄H₅₄N₂O₃
Molecular Weight:658.924
Hs Code.:

1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro<cyclohexadiene-1,3'-pyrrolidine-4',1''-cyclohexadiene>-2',4,4''-trione

Synonyms:1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione

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Chemical Property of 1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione

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Technology Process of 1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione

There total 4 articles about 1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 119507-75-4
3,5-Di-tert-butyl-N-{(3,5-di-tert-butyl-4-hydroxy-phenyl)-[(E)-p-tolylimino]-methyl}-4-hydroxy-N-p-tolyl-benzamide

: 119507-80-1
1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione

: C₄₄H₅₅N₂O₃

Guidance literature:: With hydroxide; potassium hexacyanoferrate(III); In benzene; for 8h; Ambient temperature; var.reag.: PbO₂;
DOI:10.1039/c39880000990

Reference yield: 94.0%

: 119507-75-4
N,N'-di-p-tolyl-N-(3,5-di-tert-butyl-4-hydroxybenzoyl)-3,5-di-tert-butyl-4-hydroxybenzamidine

: 119507-80-1
1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione

Guidance literature:: With potassium hydroxide; potassium hexacyanoferrate(III); In water; for 6h; Ambient temperature;

Reference yield:

: 40056-43-7
3,5-di-tert-butyl-4-hydroxybenzoyl chloride

: 119507-80-1
1'-(p-tolyl)-3,3',5,5'-tetra-tert-butyl-5'-(p-tolylimino)dispiro-2',4,4''-trione

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / benzene / 72 h / Ambient temperature

2: 94 percent / potassium ferricyanide, potassium hydroxide / H₂O / 6 h / Ambient temperature

With potassium hydroxide; potassium hexacyanoferrate(III); In water; benzene;