3-(acetylamino)-2,3,6-trideoxyhexopyranose

Base Information

• Chemical Name: 3-(acetylamino)-2,3,6-trideoxyhexopyranose
• CAS No.: 64474-85-7
• Molecular Formula: C₈H₁₅NO₄
• Molecular Weight: 189.211

Synonyms:NSC276420

Chemical Property of 3-(acetylamino)-2,3,6-trideoxyhexopyranose

Chemical Property:

• Vapor Pressure: 2.51E-10mmHg at 25°C
• Boiling Point: 458.3°C at 760 mmHg
• Flash Point: 231°C
• Density: 1.25g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(acetylamino)-2,3,6-trideoxyhexopyranose

There total 53 articles about 3-(acetylamino)-2,3,6-trideoxyhexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

methyl 3-acetamido-2,3,6-trideoxy-4-O-methoxymethyl-α-L-arabino-hexopyranoside (96796-47-3) → 3-acetamido-2,3,6-trideoxy-L-arabino-hexose (N-acetyl-L-acosamine) (23089-58-9,23089-62-5,57918-59-9,64474-85-7,72002-51-8,93303-78-7,93303-79-8,108943-61-9,108943-64-2,129172-04-9,129172-05-0,129172-06-1,129172-07-2,129172-08-3,129172-09-4)

Guidance literature:

In water; acetic acid; for 1.5h; Heating;

DOI:10.1016/0008-6215(85)85215-0

Reference yield: 83.0%

N-[(S)-3,3-Dimethoxy-1-((4S,5S)-2,2,5-trimethyl-[1,3]dioxolan-4-yl)-propyl]-acetamide (129094-44-6) → N-Acetyl-L-daunosamine (23089-58-9,23089-62-5,57918-59-9,64474-85-7,72002-51-8,93303-78-7,93303-79-8,108943-61-9,108943-64-2,129172-04-9,129172-05-0,129172-06-1,129172-07-2,129172-08-3,129172-09-4)

Guidance literature:

With acetic acid; at 100 ℃;

DOI:10.1016/S0040-4039(00)88764-X

Reference yield: 72.0%

methyl 3-acetamido-2,3,6-trideoxy-4-O-(2-methoxyethoxymethyl)-α-L-ribo-hexopyranoside (81348-15-4) → N-acetyl-L-ristosamine (23089-58-9,23089-62-5,57918-59-9,64474-85-7,72002-51-8,93303-78-7,93303-79-8,108943-61-9,108943-64-2,129172-04-9,129172-05-0,129172-06-1,129172-07-2,129172-08-3,129172-09-4)

Guidance literature:

With acetic acid; In water; for 1.5h; Heating;

upstream raw materials:

methyl 3-acetamido-2,3,6-trideoxy-4-O-(2-methoxyethoxymethyl)-α-L-ribo-hexopyranoside

methyl 3-acetamido-2,3,6-trideoxy-4-O-(methoxymethyl)-α-L-ribo-hexopyranoside

methyl 2,3-O-benzylidene-6-deoxy-α-L-mannopyranoside

methyl 2,6-dideoxy-4-O-(2-methoxyethoxymethyl)-α-L-erythro-hexopyranosid-3-ulose

Downstream raw materials:

3-acetamido-1-O-acetyl-2,3,6-trideoxy-5-O-(p-nitrobenzoyl)-D-ribo-hexofuranose

methyl 2,3,6-trideoxy-5-O-(p-nitrobenzoyl)-3-(p-nitrobenzoylacetamido)-α-D-ribo-hexofuranoside

methyl 3-acetamido-2,3,6-trideoxy-5-O-(p-nitrobenzoyl)-α-D-ribo-hexofuranoside

methyl 3-acetamido-2,3,6-trideoxy-5-O-(p-nitrobenzoyl)-β-D-ribo-hexofuranoside

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