(13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate

Base Information

Chemical Name:(13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate
CAS No.:303757-49-5
Molecular Formula:C₃₆H₄₀N₂O₇
Molecular Weight:612.723
Hs Code.:

(13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate

Synonyms:(13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate

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Chemical Property of (13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate

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Technology Process of (13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate

There total 1 articles about (13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 3-amino-6-benzyloxy-2-hydroxybenzamide

: 7698-93-3
Estradiol-17-hemisuccinate

: 303757-49-5
(13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate

Guidance literature:: With benzotriazol-1-ol; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2008.12.051

Reference yield: 76.0%

: 303757-49-5
(13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(4-benzyloxy-3-carbamoyl-2-hydroxyphenylamino)-4-oxobutanoate

: 303757-50-8
(13S,17S)-3-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl 4-(3-carbamoyl-2,4-dihydroxyphenylamino)-4-oxobutanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; ethyl acetate; for 24h; under 2068.65 Torr;
DOI:10.1016/j.bmcl.2008.12.051