3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester

Base Information

• Chemical Name: 3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester
• CAS No.: 103536-28-3
• Molecular Formula: C₂₅H₂₇NO₇
• Molecular Weight: 453.492

Synonyms:3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester

Chemical Property of 3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester

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Technology Process of 3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester

There total 2 articles about 3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thebaine (115-37-7) → 3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester (103536-28-3)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: nBu₂O / Heating

With dibutyl ether; In benzene;

DOI:10.1021/ja00894a022

Reference yield:

4,5α-epoxy-3,6-dimethoxy-17-methyl-6ξ,14ξ-etheno-morphin-7-ene-7,8-dicarboxylic acid dimethyl ester (18651-71-3) → 3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester (103536-28-3)

Guidance literature:

With dibutyl ether; Heating;

DOI:10.1021/ja00894a022

Reference yield:

3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester (103536-28-3) → 3-methoxy-6-(3-methoxy-8-methyl-6,7,8,9,10,10a-hexahydro-1H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester (103799-95-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid;

DOI:10.1021/ja00894a022

upstream raw materials:

4,5α-epoxy-3,6-dimethoxy-17-methyl-6ξ,14ξ-etheno-morphin-7-ene-7,8-dicarboxylic acid dimethyl ester

thebaine

Downstream raw materials:

[3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol

3-methoxy-6-(3-methoxy-8-methyl-6,7,8,9,10,10a-hexahydro-1H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester

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