N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide

Base Information

Chemical Name:N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide
CAS No.:1638254-76-8
Molecular Formula:C₂₂H₂₆ClN₃O₂
Molecular Weight:399.92
Hs Code.:

Synonyms:N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide

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Chemical Property of N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide

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Technology Process of N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide

There total 5 articles about N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1610368-79-0
N-(4-(hydrazinecarbonyl)phenyl)-2-propylpentanamide

: 104-88-1
4-chlorobenzaldehyde

: 1638254-76-8
N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide

Guidance literature:: With acetic acid; In methanol; for 8h; Reflux;
DOI:10.1248/cpb.c14-00143

Reference yield:

: 690988-44-4
ethyl 4-(2-propylpentanamido)benzoate

: 1638254-76-8
N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / methanol / 4 h / Reflux

2: acetic acid / methanol / 8 h / Reflux

With acetic acid; hydrazine; In methanol;
DOI:10.1248/cpb.c14-00143

Reference yield:

: 99-66-1
valproic acid

: 1638254-76-8
N-(4-(2-4-chlorobenzylidenehydrazinecarbonyl)phenyl)-2-propylpentanamide

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: triethylamine / dichloromethane / 0 - 20 °C

3: hydrazine / methanol / 4 h / Reflux

4: acetic acid / methanol / 8 h / Reflux

With thionyl chloride; acetic acid; triethylamine; hydrazine; In methanol; dichloromethane;
DOI:10.1248/cpb.c14-00143