2-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-9-ethyl-heptafluorophosphafluorene

Base Information

Chemical Name:2-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-9-ethyl-heptafluorophosphafluorene
CAS No.:1219681-08-9
Molecular Formula:C₃₈H₂₂F₁₁OPS₂
Molecular Weight:798.68
Hs Code.:

Synonyms:2-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-9-ethyl-heptafluorophosphafluorene

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Chemical Property of 2-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-9-ethyl-heptafluorophosphafluorene

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Technology Process of 2-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-9-ethyl-heptafluorophosphafluorene

There total 1 articles about 2-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-9-ethyl-heptafluorophosphafluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: dichloroethylphosphine

: 1219680-98-4
2,2'-dibromo-4-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-heptafluorobiphenyl

: 1219681-08-9
2-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-9-ethyl-heptafluorophosphafluorene

Guidance literature:: 2,2'-dibromo-4-(1-(5-ethynyl-5'-hexyl-2,2'-bithienyl)-4-ethynyltetrafluorophenyl)-heptafluorobiphenyl; With n-butyllithium; In diethyl ether; hexane; toluene; at -78 ℃; for 0.333333h;

dichloroethylphosphine; at -78 - 20 ℃; for 12h;

With dihydrogen peroxide; In tetrahydrofuran; water; for 4h;
DOI:10.1021/jo902488w