methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate

Base Information

Chemical Name:methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate
CAS No.:1415904-95-8
Molecular Formula:C₁₉H₂₃IO₆
Molecular Weight:474.293
Hs Code.:

Synonyms:methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate

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Chemical Property of methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate

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Technology Process of methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate

There total 2 articles about methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1415904-94-7
methyl 2-((E)-2-((3aS,4S,6R,6aR)-6-(hydroxymethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate

: 1415904-95-8
methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 2.25h;
DOI:10.1016/j.tetasy.2012.10.010

Reference yield:

: C₂₅H₃₈O₇Si

: 1415904-95-8
methyl 2-((E)-2-((3aS,4S,6S,6aS)-6-(iodomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinyl)-6-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.17 h / 0 - 20 °C

2: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 2.25 h / 0 - 20 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; iodine; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2012.10.010