1-chlorodecanyl p-tolyl sulfoxide

Base Information

Chemical Name:1-chlorodecanyl p-tolyl sulfoxide
CAS No.:119487-93-3
Molecular Formula:C₁₈H₂₉ClOS
Molecular Weight:328.947
Hs Code.:

Synonyms:1-chlorodecanyl p-tolyl sulfoxide

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Chemical Property of 1-chlorodecanyl p-tolyl sulfoxide

Chemical Property:

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Technology Process of 1-chlorodecanyl p-tolyl sulfoxide

There total 3 articles about 1-chlorodecanyl p-tolyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1519-39-7
(R)-methyl p-tolyl sulfoxide

: 116386-54-0,116386-55-1,119487-93-3
(-)-1-chloroundecyl p-tolyl sulfoxide

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃, N-chlorosuccinimide (NCS) / CH₂Cl₂ / 40 h / Ambient temperature

2: 1.) lithium diisopropylamide (LDA) / 1.) THF, -60 deg C, 25 min, 2.) from -60 deg C to -20 deg C, 1 h

With N-chloro-succinimide; potassium carbonate; lithium diisopropyl amide; In dichloromethane;
DOI:10.1021/jo00274a032

Reference yield:

: 1517-82-4
(-)-menthyl p-toluenesulfinate

: 116386-54-0,116386-55-1,119487-93-3
(-)-1-chloroundecyl p-tolyl sulfoxide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / toluene / -60 - -20 °C

2: K₂CO₃, N-chlorosuccinimide (NCS) / CH₂Cl₂ / 40 h / Ambient temperature

3: 1.) lithium diisopropylamide (LDA) / 1.) THF, -60 deg C, 25 min, 2.) from -60 deg C to -20 deg C, 1 h

With N-chloro-succinimide; potassium carbonate; lithium diisopropyl amide; In dichloromethane; toluene;
DOI:10.1021/jo00274a032

Reference yield:

: 2050-77-3
Iododecane

: 31350-91-1
(R)-chloromethyl p-tolyl sulfoxide

: 116386-54-0,116386-55-1,119487-93-3
(-)-1-chloroundecyl p-tolyl sulfoxide

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -60 deg C, 25 min, 2.) from -60 deg C to -20 deg C, 1 h;
DOI:10.1021/jo00274a032