methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate

Base Information

Chemical Name:methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate
CAS No.:883908-39-2
Molecular Formula:C₂₂H₂₄N₂O₃S
Molecular Weight:396.51
Hs Code.:

Synonyms:methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate

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Technology Process of methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate

There total 1 articles about methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 26567-78-2
(Z)-4-(phenylamino)-3-penten-2-one

: 88576-93-6,147091-08-5
(S)-2-isothiocyanato-3-phenylpropionic acid methyl ester

: 883908-39-2
methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate

Guidance literature:: at 90 ℃; for 1h;
DOI:10.1007/s00706-005-0353-4

Reference yield: 85.0%

: 883908-39-2
methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate

: 883908-44-9
methyl (S)-(+)-3-phenyl-2-((Z)-3-(phenylamino)but-2-enethioylamino)propionate

Guidance literature:: With sodium hydrogencarbonate; In methanol; for 1.5h; Heating;
DOI:10.1007/s00706-005-0353-4

Reference yield:

: 883908-39-2
methyl (S)-(+)-2-((E)-2-acetyl-3-(phenylamino)but-2-enethioylamino)-3-phenylpropionate

: methyl (S)-(-)-2-(3-methyl-2-phenyl-2H-isothiazol-(5Z)-ylideneamino)-3-phenylpropionate hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaHCO₃ / methanol / 1.5 h / Heating

2: 75 percent / Br₂ / CHCl₃ / 0 - 20 °C

With bromine; sodium hydrogencarbonate; In methanol; chloroform;
DOI:10.1007/s00706-005-0353-4