3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester

Base Information

Chemical Name:3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester
CAS No.:206053-73-8
Molecular Formula:C₄₁H₄₆O₁₀
Molecular Weight:698.81
Hs Code.:

Synonyms:3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester

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Chemical Property of 3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester

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Technology Process of 3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester

There total 3 articles about 3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 96-32-2
bromoacetic acid methyl ester

: 206053-72-7
3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-hydroxybenzoic acid methyl ester

: 206053-73-8
3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 5h;
DOI:10.1016/S0040-4020(98)00105-7

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 206053-73-8
3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃ / dimethylformamide / 1.) 0 deg C, 12 h, 2.) 20 deg C, 24 h

2: 84 percent / K₂CO₃ / dimethylformamide / 5 h / 50 °C

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(98)00105-7

Reference yield:

: 181629-30-1
3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyl bromide

: 206053-73-8
3-[3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyloxy]-5-methoxycarbonylphenoxyacetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃ / dimethylformamide / 1.) 0 deg C, 12 h, 2.) 20 deg C, 24 h

2: 84 percent / K₂CO₃ / dimethylformamide / 5 h / 50 °C

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(98)00105-7