(R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol

Base Information

Chemical Name:(R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol
CAS No.:1005002-00-5
Molecular Formula:C₂₄H₁₈F₉NO₄S
Molecular Weight:587.463
Hs Code.:

Synonyms:(R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol

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Chemical Property of (R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol

Chemical Property:

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Technology Process of (R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol

There total 3 articles about (R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1005002-02-7
(R)-2-amino-2-(4-hydroxyphenyl)-1,1-diphenylethanol

: 375-72-4
Nonafluorobutanesulfonyl fluoride

: 1005002-00-5
(R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol

Guidance literature:: (R)-2-amino-2-(4-hydroxyphenyl)-1,1-diphenylethanol; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 3h;

Nonafluorobutanesulfonyl fluoride; In N,N-dimethyl-formamide; at 20 ℃; Further stages.;
DOI:10.1002/adsc.200600297

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1005002-00-5
(R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg turnings; iodine / tetrahydrofuran / 1 h / Heating

1.2: 48 percent / tetrahydrofuran / 20 h / 0 °C

2.1: NaH / dimethylformamide / 3 h / 0 °C

2.2: 74 percent / dimethylformamide / 20 °C

With iodine; sodium hydride; magnesium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/adsc.200600297

Reference yield:

: 57591-61-4,68697-60-9,127369-30-6,134694-94-3
methyl (R)-2-amino-2-(4-hydroxyphenyl)acetate hydrochloride

: 1005002-00-5
(R)-2-amino-2-[4-(nonafluorobutanesulfonyloxy)phenyl]-1,1-diphenylethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg turnings; iodine / tetrahydrofuran / 1 h / Heating

1.2: 48 percent / tetrahydrofuran / 20 h / 0 °C

2.1: NaH / dimethylformamide / 3 h / 0 °C

2.2: 74 percent / dimethylformamide / 20 °C

With iodine; sodium hydride; magnesium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/adsc.200600297