BocHN-(R)^β-CbzHNγ-Im-CO2Et

Base Information

• Chemical Name: BocHN-(R)^β-CbzHNγ-Im-CO2Et
• CAS No.: 1158186-73-2
• Molecular Formula: C₂₄H₃₃N₅O₇
• Molecular Weight: 503.555
• Mol file: 1158186-73-2.mol

Synonyms:BocHN-(R)^β-CbzHNγ-Im-CO2Et

Chemical Property of BocHN-(R)^β-CbzHNγ-Im-CO2Et

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of BocHN-(R)^β-CbzHNγ-Im-CO2Et

There total 1 articles about BocHN-(R)^β-CbzHNγ-Im-CO2Et which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

HCl *H2N-Im-CO2Et + L-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyric acid (108919-51-3) → BocHN-(R)β-CbzHNγ-Im-CO2Et (1158186-73-2)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 23 ℃; for 8h;

Reference yield: 99.0%

BocHN-(R)β-CbzHNγ-Im-CO2Et (1158186-73-2) → HCl*H2N-(R)β-CbzHNγ-Im-CO2Et (1158186-74-3)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 23 ℃; for 16h;

Reference yield: 95.0%

BocHN-(R)β-CbzHNγ-Im-CO2Et (1158186-73-2) → BocHN-(R)β-CbzHNγ-Im-CO2H (1158208-55-9)

Guidance literature:

BocHN-(R)^β-CbzHNγ-Im-CO2Et; With potassium hydroxide; In methanol; water; at 37 ℃; for 2h;

With hydrogenchloride; In methanol; water; Cooling with ice;

upstream raw materials:

L-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyric acid

Downstream raw materials:

HCl*H2N-(R)^β-CbzHNγ-Im-CO2Et

BocHN-(R)β-CbzHNγ-Im-CO2H