(5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine

Base Information

• Chemical Name: (5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine
• CAS No.: 1206156-37-7
• Molecular Formula: C₁₄H₂₆N₂OSi
• Molecular Weight: 266.459
• Mol file: 1206156-37-7.mol

Synonyms:(5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine

Chemical Property of (5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine

Chemical Property:

Purity/Quality:

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Technology Process of (5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine

There total 1 articles about (5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

2,2'-(5-(tert-butyldimethylsilyloxy)-1,3-phenylene)bis(methylene)diisoindoline-1,3-dione (1055309-13-1) → (5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine (1206156-37-7)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Reflux;

DOI:10.1080/10610278.2012.671523

Reference yield: 64.0%

(5-(tert-butyldimethylsilyloxy)-1,3-phenylene)dimethanamine (1206156-37-7) + 2,5-dioxopyrrolidin-1-yl 5-(butylcarbamoyl)-1Hpyrrole-2-carboxylate (1408284-23-0) → N2,N2'-(5-(tert-butyldimethylsilyloxy)-1,3-phenylene) bis(methylene)bis(N5-butyl-1H-pyrrole-2,5-dicarboxamide) (1408284-24-1)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 19h; Inert atmosphere;

DOI:10.1080/10610278.2012.671523

upstream raw materials:

2,2'-(5-(tert-butyldimethylsilyloxy)-1,3-phenylene)bis(methylene)diisoindoline-1,3-dione

Downstream raw materials:

N₂,N₂'-(5-(tert-butyldimethylsilyloxy)-1,3-phenylene) bis(methylene)bis(N₅-butyl-1H-pyrrole-2,5-dicarboxamide)