4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester

Base Information

Chemical Name:4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester
CAS No.:187801-06-5
Molecular Formula:C₁₇H₂₄O₂Si
Molecular Weight:288.462
Hs Code.:

Synonyms:4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester

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Chemical Property of 4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester

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Technology Process of 4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester

There total 3 articles about 4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 187800-99-3
Dimethyl-(2-methylene-but-3-enyl)-phenyl-silane

: 187801-06-5
4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester

Guidance literature:: With dimethylaluminum chloride; In dichloromethane; at 40 ℃;
DOI:10.1021/jo970821v

Reference yield:

: 107735-20-6
[(dimethylphenylsilyl)methyl]magnesium chloride

: 187801-06-5
4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / <1,3-bis(diphenylphosphino)propane>dichloronickel / diethyl ether / 5 h / Heating

2: 84 percent / Me₂AlCl / CH₂Cl₂ / 4.5 h / Heating

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); dimethylaluminum chloride; In diethyl ether; dichloromethane;
DOI:10.1021/jo962025f

Reference yield:

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 187800-99-3
Dimethyl-(2-methylene-but-3-enyl)-phenyl-silane

: 71092-50-7
methyl 4-methylenecyclohexane carboxylate

: 187801-06-5
4-[(Dimethyl-phenyl-silanyl)-methyl]-cyclohex-3-enecarboxylic acid methyl ester

Guidance literature:: With titanium tetrachloride; sodium hydrogencarbonate; Multistep reaction. Title compound not separated from byproducts; 1) CD₂Cl₂, 18 h, 2) CD₂Cl₂;
DOI:10.1021/jo970821v